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result sql = A method for the determination of some pesticide residues in must and wine samples was developed using solid-phase microextraction (SPME) and gas chromatography-electron capture detection (GC/ECD). The procedure only needs dilution as sample pre-treatment and is therefore simple, fast and solvent-free. Eight fungicides (vinclozolin, procymidone, iprodione, penconazole, fenarimol, folpet, nuarimol and hexaconazole), one insecticide (chlorpyriphos) and two acaricides (bromopropylate and tetradifon) can be quantified. Good linearity was observed for all the compounds in the range 5-100 microg/L. The reproducibility of the measurements was found acceptable (with RSD's below 20%). Detection limits of 11 microg/L, on average, are sufficiently below the proposed maximum residue limits (MRL's) for these compounds in wine. The analytical method was applied to the determination of these compounds in Portuguese must and wine samples from the Demarcated Region of Alentejo, where any residues could be detected.
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result sql = Development of a SPME-GC-ECD methodology for selected pesticides in must and wine samples.
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char = m;code = 109
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char = m;code = 109
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char = w;code = 119
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char = n;code = 110
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char = ;code = 32
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char = p;code = 112
char = l;code = 108
char = i;code = 105
char = e;code = 101
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char = ;code = 32
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char = D;code = 68
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char = c;code = 99
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char = e;code = 101
char = d;code = 100
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char = R;code = 82
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char = e;code = 101
char = ;code = 32
char = d;code = 100
char = e;code = 101
char = t;code = 116
char = e;code = 101
char = c;code = 99
char = t;code = 116
char = e;code = 101
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result sql = A method for the determination of some pesticide residues in must and wine samples was developed using solid-phase microextraction (SPME) and gas chromatography-electron capture detection (GC/ECD). The procedure only needs dilution as sample pre-treatment and is therefore simple, fast and solvent-free. Eight fungicides (vinclozolin, procymidone, iprodione, penconazole, fenarimol, folpet, nuarimol and hexaconazole), one insecticide (chlorpyriphos) and two acaricides (bromopropylate and tetradifon) can be quantified. Good linearity was observed for all the compounds in the range 5-100 microg/L. The reproducibility of the measurements was found acceptable (with RSD's below 20%). Detection limits of 11 microg/L, on average, are sufficiently below the proposed maximum residue limits (MRL's) for these compounds in wine. The analytical method was applied to the determination of these compounds in Portuguese must and wine samples from the Demarcated Region of Alentejo, where any residues could be detected.
Publication: Fresenius J Anal Chem 2001 Apr ;369(7-8)::647-51.
Publication Date: 2001 Apr
Study Author(s): Correia, M;Delerue-Matos, C;Alves, A;
Institution: Laboratório de Engenharia de Processos, Ambiente e Energia, Faculdade de Engenharia da Universidade do Porto, Portugal.
Shortcut link to this study:
Publication Date: 2001 Apr
Study Author(s): Correia, M;Delerue-Matos, C;Alves, A;
Institution: Laboratório de Engenharia de Processos, Ambiente e Energia, Faculdade de Engenharia da Universidade do Porto, Portugal.
Shortcut link to this study:
A method for the determination of some pesticide residues in must and wine samples was developed using solid-phase microextraction (SPME) and gas chromatography-electron capture detection (GC/ECD). The procedure only needs dilution as sample pre-treatment and is therefore simple, fast and solvent-free. Eight fungicides (vinclozolin, procymidone, iprodione, penconazole, fenarimol, folpet, nuarimol and hexaconazole), one insecticide (chlorpyriphos) and two acaricides (bromopropylate and tetradifon) can be quantified. Good linearity was observed for all the compounds in the range 5-100 microg/L. The reproducibility of the measurements was found acceptable (with RSD's below 20%). Detection limits of 11 microg/L, on average, are sufficiently below the proposed maximum residue limits (MRL's) for these compounds in wine. The analytical method was applied to the determination of these compounds in Portuguese must and wine samples from the Demarcated Region of Alentejo, where any residues could be detected.
PMID: 11371065
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