char = m;code = 109 char = u;code = 117 char = -;code = 45 char = O;code = 79 char = x;code = 120 char = o;code = 111 char = -;code = 45 char = b;code = 98 char = i;code = 105 char = s;code = 115 char = {;code = 123 char = [;code = 91 char = (;code = 40 char = 6;code = 54 char = -;code = 45 char = h;code = 104 char = y;code = 121 char = d;code = 100 char = r;code = 114 char = o;code = 111 char = x;code = 120 char = y;code = 121 char = m;code = 109 char = e;code = 101 char = t;code = 116 char = h;code = 104 char = y;code = 121 char = l;code = 108 char = -;code = 45 char = 2;code = 50 char = -;code = 45 char = p;code = 112 char = y;code = 121 char = r;code = 114 char = i;code = 105 char = d;code = 100 char = y;code = 121 char = l;code = 108 char = m;code = 109 char = e;code = 101 char = t;code = 116 char = h;code = 104 char = y;code = 121 char = l;code = 108 char = );code = 41 char = b;code = 98 char = i;code = 105 char = s;code = 115 char = (;code = 40 char = 2;code = 50 char = -;code = 45 char = p;code = 112 char = y;code = 121 char = r;code = 114 char = i;code = 105 char = d;code = 100 char = y;code = 121 char = l;code = 108 char = m;code = 109 char = e;code = 101 char = t;code = 116 char = h;code = 104 char = y;code = 121 char = l;code = 108 char = );code = 41 char = a;code = 97 char = m;code = 109 char = i;code = 105 char = n;code = 110 char = e;code = 101 char = -;code = 45 char = k;code = 107 char = a;code = 97 char = p;code = 112 char = p;code = 112 char = a;code = 97 char = );code = 41 char = N;code = 78 char = ,;code = 44 char = N;code = 78 char = ';code = 39 char = ,;code = 44 char = N;code = 78 char = ';code = 39 char = ';code = 39 char = ,;code = 44 char = N;code = 78 char = ';code = 39 char = ';code = 39 char = ';code = 39 char = ,;code = 44 char = O;code = 79 char = ];code = 93 char = i;code = 105 char = r;code = 114 char = o;code = 111 char = n;code = 110 char = (;code = 40 char = I;code = 73 char = I;code = 73 char = I;code = 73 char = );code = 41 char = };code = 125 char = ;code = 32 char = t;code = 116 char = e;code = 101 char = t;code = 116 char = r;code = 114 char = a;code = 97 char = k;code = 107 char = i;code = 105 char = s;code = 115 char = (;code = 40 char = p;code = 112 char = e;code = 101 char = r;code = 114 char = c;code = 99 char = h;code = 104 char = l;code = 108 char = o;code = 111 char = r;code = 114 char = a;code = 97 char = t;code = 116 char = e;code = 101 char = );code = 41 char = .;code = 46 result sql = mu-Oxo-bis{[(6-hydroxymethyl-2-pyridylmethyl)bis(2-pyridylmethyl)amine-kappa)N,N',N'',N''',O]iron(III)} tetrakis(perchlorate).
mu-Oxo-bis{[(6-hydroxymethyl-2-pyridylmethyl)bis(2-pyridylmethyl)amine-kappa)N,N',N'',N''',O]iron(III)} tetrakis(perchlorate).char = T;code = 84 char = h;code = 104 char = e;code = 101 char = ;code = 32 char = n;code = 110 char = o;code = 111 char = v;code = 118 char = e;code = 101 char = l;code = 108 char = ;code = 32 char = m;code = 109 char = u;code = 117 char = -;code = 45 char = o;code = 111 char = x;code = 120 char = o;code = 111 char = -;code = 45 char = d;code = 100 char = i;code = 105 char = i;code = 105 char = r;code = 114 char = o;code = 111 char = n;code = 110 char = ;code = 32 char = c;code = 99 char = o;code = 111 char = m;code = 109 char = p;code = 112 char = l;code = 108 char = e;code = 101 char = x;code = 120 char = ;code = 32 char = [;code = 91 char = F;code = 70 char = e;code = 101 char = 2;code = 50 char = O;code = 79 char = (;code = 40 char = B;code = 66 char = P;code = 80 char = H;code = 72 char = P;code = 80 char = A;code = 65 char = );code = 41 char = 2;code = 50 char = ];code = 93 char = (;code = 40 char = C;code = 67 char = l;code = 108 char = O;code = 79 char = 4;code = 52 char = );code = 41 char = 4;code = 52 char = ;code = 32 char = [;code = 91 char = B;code = 66 char = P;code = 80 char = H;code = 72 char = P;code = 80 char = A;code = 65 char = ;code = 32 char = i;code = 105 char = s;code = 115 char = ;code = 32 char = (;code = 40 char = 6;code = 54 char = -;code = 45 char = h;code = 104 char = y;code = 121 char = d;code = 100 char = r;code = 114 char = o;code = 111 char = x;code = 120 char = y;code = 121 char = m;code = 109 char = e;code = 101 char = t;code = 116 char = h;code = 104 char = y;code = 121 char = l;code = 108 char = -;code = 45 char = 2;code = 50 char = -;code = 45 char = p;code = 112 char = y;code = 121 char = r;code = 114 char = i;code = 105 char = d;code = 100 char = y;code = 121 char = l;code = 108 char = m;code = 109 char = e;code = 101 char = t;code = 116 char = h;code = 104 char = y;code = 121 char = l;code = 108 char = );code = 41 char = b;code = 98 char = i;code = 105 char = s;code = 115 char = (;code = 40 char = 2;code = 50 char = -;code = 45 char = p;code = 112 char = y;code = 121 char = r;code = 114 char = i;code = 105 char = d;code = 100 char = y;code = 121 char = l;code = 108 char = m;code = 109 char = e;code = 101 char = t;code = 116 char = h;code = 104 char = y;code = 121 char = l;code = 108 char = );code = 41 char = a;code = 97 char = m;code = 109 char = i;code = 105 char = n;code = 110 char = e;code = 101 char = ,;code = 44 char = ;code = 32 char = C;code = 67 char = 1;code = 49 char = 9;code = 57 char = H;code = 72 char = 2;code = 50 char = 0;code = 48 char = N;code = 78 char = 4;code = 52 char = O;code = 79 char = ];code = 93 char = ,;code = 44 char = ;code = 32 char = c;code = 99 char = o;code = 111 char = n;code = 110 char = t;code = 116 char = a;code = 97 char = i;code = 105 char = n;code = 110 char = s;code = 115 char = ;code = 32 char = a;code = 97 char = ;code = 32 char = b;code = 98 char = i;code = 105 char = n;code = 110 char = u;code = 117 char = c;code = 99 char = l;code = 108 char = e;code = 101 char = a;code = 97 char = r;code = 114 char = ;code = 32 char = c;code = 99 char = e;code = 101 char = n;code = 110 char = t;code = 116 char = r;code = 114 char = o;code = 111 char = s;code = 115 char = y;code = 121 char = m;code = 109 char = m;code = 109 char = e;code = 101 char = t;code = 116 char = r;code = 114 char = i;code = 105 char = c;code = 99 char = ;code = 32 char = [;code = 91 char = F;code = 70 char = e;code = 101 char = 2;code = 50 char = O;code = 79 char = (;code = 40 char = B;code = 66 char = P;code = 80 char = H;code = 72 char = P;code = 80 char = A;code = 65 char = );code = 41 char = 2;code = 50 char = ];code = 93 char = 4;code = 52 char = +;code = 43 char = ;code = 32 char = c;code = 99 char = a;code = 97 char = t;code = 116 char = i;code = 105 char = o;code = 111 char = n;code = 110 char = ;code = 32 char = (;code = 40 char = t;code = 116 char = h;code = 104 char = e;code = 101 char = ;code = 32 char = b;code = 98 char = r;code = 114 char = i;code = 105 char = d;code = 100 char = g;code = 103 char = i;code = 105 char = n;code = 110 char = g;code = 103 char = ;code = 32 char = O;code = 79 char = ;code = 32 char = a;code = 97 char = t;code = 116 char = o;code = 111 char = m;code = 109 char = ;code = 32 char = l;code = 108 char = i;code = 105 char = e;code = 101 char = s;code = 115 char = ;code = 32 char = o;code = 111 char = n;code = 110 char = ;code = 32 char = a;code = 97 char = n;code = 110 char = ;code = 32 char = i;code = 105 char = n;code = 110 char = v;code = 118 char = e;code = 101 char = r;code = 114 char = s;code = 115 char = i;code = 105 char = o;code = 111 char = n;code = 110 char = ;code = 32 char = c;code = 99 char = e;code = 101 char = n;code = 110 char = t;code = 116 char = r;code = 114 char = e;code = 101 char = );code = 41 char = ;code = 32 char = a;code = 97 char = n;code = 110 char = d;code = 100 char = ;code = 32 char = f;code = 102 char = o;code = 111 char = u;code = 117 char = r;code = 114 char = ;code = 32 char = p;code = 112 char = e;code = 101 char = r;code = 114 char = c;code = 99 char = h;code = 104 char = l;code = 108 char = o;code = 111 char = r;code = 114 char = a;code = 97 char = t;code = 116 char = e;code = 101 char = ;code = 32 char = a;code = 97 char = n;code = 110 char = i;code = 105 char = o;code = 111 char = n;code = 110 char = s;code = 115 char = .;code = 46 char = ;code = 32 char = E;code = 69 char = a;code = 97 char = c;code = 99 char = h;code = 104 char = ;code = 32 char = i;code = 105 char = r;code = 114 char = o;code = 111 char = n;code = 110 char = ;code = 32 char = i;code = 105 char = o;code = 111 char = n;code = 110 char = ;code = 32 char = i;code = 105 char = s;code = 115 char = ;code = 32 char = c;code = 99 char = o;code = 111 char = o;code = 111 char = r;code = 114 char = d;code = 100 char = i;code = 105 char = n;code = 110 char = a;code = 97 char = t;code = 116 char = e;code = 101 char = d;code = 100 char = ;code = 32 char = b;code = 98 char = y;code = 121 char = ;code = 32 char = f;code = 102 char = o;code = 111 char = u;code = 117 char = r;code = 114 char = ;code = 32 char = N;code = 78 char = ;code = 32 char = a;code = 97 char = t;code = 116 char = o;code = 111 char = m;code = 109 char = s;code = 115 char = ;code = 32 char = [;code = 91 char = F;code = 70 char = e;code = 101 char = -;code = 45 char = N;code = 78 char = ;code = 32 char = =;code = 61 char = ;code = 32 char = 2;code = 50 char = .;code = 46 char = 1;code = 49 char = 1;code = 49 char = 7;code = 55 char = ;code = 32 char = (;code = 40 char = 5;code = 53 char = );code = 41 char = -;code = 45 char = 2;code = 50 char = .;code = 46 char = 1;code = 49 char = 9;code = 57 char = 6;code = 54 char = ;code = 32 char = (;code = 40 char = 5;code = 53 char = );code = 41 char = ;code = 32 char = A;code = 65 char = ];code = 93 char = ;code = 32 char = a;code = 97 char = n;code = 110 char = d;code = 100 char = ;code = 32 char = o;code = 111 char = n;code = 110 char = e;code = 101 char = ;code = 32 char = O;code = 79 char = ;code = 32 char = a;code = 97 char = t;code = 116 char = o;code = 111 char = m;code = 109 char = ;code = 32 char = [;code = 91 char = F;code = 70 char = e;code = 101 char = -;code = 45 char = O;code = 79 char = ;code = 32 char = =;code = 61 char = ;code = 32 char = 2;code = 50 char = .;code = 46 char = 0;code = 48 char = 5;code = 53 char = 2;code = 50 char = ;code = 32 char = (;code = 40 char = 5;code = 53 char = );code = 41 char = ;code = 32 char = A;code = 65 char = ];code = 93 char = ;code = 32 char = f;code = 102 char = r;code = 114 char = o;code = 111 char = m;code = 109 char = ;code = 32 char = a;code = 97 char = ;code = 32 char = B;code = 66 char = P;code = 80 char = H;code = 72 char = P;code = 80 char = A;code = 65 char = ;code = 32 char = l;code = 108 char = i;code = 105 char = g;code = 103 char = a;code = 97 char = n;code = 110 char = d;code = 100 char = ,;code = 44 char = ;code = 32 char = a;code = 97 char = n;code = 110 char = d;code = 100 char = ;code = 32 char = b;code = 98 char = y;code = 121 char = ;code = 32 char = o;code = 111 char = n;code = 110 char = e;code = 101 char = ;code = 32 char = b;code = 98 char = r;code = 114 char = i;code = 105 char = d;code = 100 char = g;code = 103 char = i;code = 105 char = n;code = 110 char = g;code = 103 char = ;code = 32 char = o;code = 111 char = x;code = 120 char = o;code = 111 char = ;code = 32 char = a;code = 97 char = t;code = 116 char = o;code = 111 char = m;code = 109 char = ;code = 32 char = [;code = 91 char = F;code = 70 char = e;code = 101 char = -;code = 45 char = O;code = 79 char = ;code = 32 char = =;code = 61 char = ;code = 32 char = 1;code = 49 char = .;code = 46 char = 7;code = 55 char = 8;code = 56 char = 9;code = 57 char = 6;code = 54 char = ;code = 32 char = (;code = 40 char = 9;code = 57 char = );code = 41 char = ;code = 32 char = A;code = 65 char = ];code = 93 char = ,;code = 44 char = ;code = 32 char = f;code = 102 char = o;code = 111 char = r;code = 114 char = m;code = 109 char = i;code = 105 char = n;code = 110 char = g;code = 103 char = ;code = 32 char = a;code = 97 char = ;code = 32 char = d;code = 100 char = i;code = 105 char = s;code = 115 char = t;code = 116 char = o;code = 111 char = r;code = 114 char = t;code = 116 char = e;code = 101 char = d;code = 100 char = ;code = 32 char = o;code = 111 char = c;code = 99 char = t;code = 116 char = a;code = 97 char = h;code = 104 char = e;code = 101 char = d;code = 100 char = r;code = 114 char = o;code = 111 char = n;code = 110 char = .;code = 46 char = ;code = 32 char = T;code = 84 char = h;code = 104 char = e;code = 101 char = r;code = 114 char = e;code = 101 char = ;code = 32 char = a;code = 97 char = r;code = 114 char = e;code = 101 char = ;code = 32 char = h;code = 104 char = y;code = 121 char = d;code = 100 char = r;code = 114 char = o;code = 111 char = g;code = 103 char = e;code = 101 char = n;code = 110 char = ;code = 32 char = b;code = 98 char = o;code = 111 char = n;code = 110 char = d;code = 100 char = s;code = 115 char = ;code = 32 char = b;code = 98 char = e;code = 101 char = t;code = 116 char = w;code = 119 char = e;code = 101 char = e;code = 101 char = n;code = 110 char = ;code = 32 char = t;code = 116 char = h;code = 104 char = e;code = 101 char = ;code = 32 char = h;code = 104 char = y;code = 121 char = d;code = 100 char = r;code = 114 char = o;code = 111 char = x;code = 120 char = y;code = 121 char = ;code = 32 char = g;code = 103 char = r;code = 114 char = o;code = 111 char = u;code = 117 char = p;code = 112 char = ;code = 32 char = a;code = 97 char = n;code = 110 char = d;code = 100 char = ;code = 32 char = p;code = 112 char = e;code = 101 char = r;code = 114 char = c;code = 99 char = h;code = 104 char = l;code = 108 char = o;code = 111 char = r;code = 114 char = a;code = 97 char = t;code = 116 char = e;code = 101 char = ;code = 32 char = O;code = 79 char = ;code = 32 char = a;code = 97 char = t;code = 116 char = o;code = 111 char = m;code = 109 char = s;code = 115 char = ;code = 32 char = [;code = 91 char = O;code = 79 char = -;code = 45 char = H;code = 72 char = .;code = 46 char = .;code = 46 char = .;code = 46 char = O;code = 79 char = ;code = 32 char = =;code = 61 char = ;code = 32 char = 2;code = 50 char = .;code = 46 char = 6;code = 54 char = 5;code = 53 char = 4;code = 52 char = ;code = 32 char = (;code = 40 char = 7;code = 55 char = );code = 41 char = ;code = 32 char = A;code = 65 char = ];code = 93 char = .;code = 46 char = <;code = 60 char = b;code = 98 char = r;code = 114 char = /;code = 47 char = >;code = 62 result sql = The novel mu-oxo-diiron complex [Fe2O(BPHPA)2](ClO4)4 [BPHPA is (6-hydroxymethyl-2-pyridylmethyl)bis(2-pyridylmethyl)amine, C19H20N4O], contains a binuclear centrosymmetric [Fe2O(BPHPA)2]4+ cation (the bridging O atom lies on an inversion centre) and four perchlorate anions. Each iron ion is coordinated by four N atoms [Fe-N = 2.117 (5)-2.196 (5) A] and one O atom [Fe-O = 2.052 (5) A] from a BPHPA ligand, and by one bridging oxo atom [Fe-O = 1.7896 (9) A], forming a distorted octahedron. There are hydrogen bonds between the hydroxy group and perchlorate O atoms [O-H...O = 2.654 (7) A].
Publication: Acta Crystallogr C 2005 Jan ;61(Pt 1)::m13-5.
Publication Date: 2005 Jan
Study Author(s): Gao, Yun-Ling;Peng, Xiao-Jun;Sun, Shi-Guo;Chen, Chang-Neng;
Institution: State Key Laboratory of Fine Chemicals, Dalian University of Technology, Dalian, Liaoning 116012, People's Republic of China.
Shortcut link to this study:
The novel mu-oxo-diiron complex [Fe2O(BPHPA)2](ClO4)4 [BPHPA is (6-hydroxymethyl-2-pyridylmethyl)bis(2-pyridylmethyl)amine, C19H20N4O], contains a binuclear centrosymmetric [Fe2O(BPHPA)2]4+ cation (the bridging O atom lies on an inversion centre) and four perchlorate anions. Each iron ion is coordinated by four N atoms [Fe-N = 2.117 (5)-2.196 (5) A] and one O atom [Fe-O = 2.052 (5) A] from a BPHPA ligand, and by one bridging oxo atom [Fe-O = 1.7896 (9) A], forming a distorted octahedron. There are hydrogen bonds between the hydroxy group and perchlorate O atoms [O-H...O = 2.654 (7) A].
PMID: 15640566